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International Journal of Refractory Metals and Hard Materials | Vol.90, Issue. | 2020-07-31 | Pages 105234

International Journal of Refractory Metals and Hard Materials

Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT)

Mayara Adrielly Leal de Oliveira Rodrigues   Lucas Pires de Paiva Barreto   Uílame Umbelino Gomes   Marcello Filgueira   Diego Pires Gurgel   Lukas Bichler   Meysam Mashhadikarimi  
Abstract

In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revealed a uniform dispersion of the Nb additives in the diamond matrix and no interfacial cracking was observed. Higher concentration of binder increased tendency to intergranular failure. The formation of NbC and NbC0.84 phases after sintering was identified, indicating that some of the matrix carbon may have undergone graphitization.

Original Text (This is the original text for your reference.)

Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT)

In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revealed a uniform dispersion of the Nb additives in the diamond matrix and no interfacial cracking was observed. Higher concentration of binder increased tendency to intergranular failure. The formation of NbC and NbC0.84 phases after sintering was identified, indicating that some of the matrix carbon may have undergone graphitization.

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Mayara Adrielly Leal de Oliveira Rodrigues, Lucas Pires de Paiva Barreto, Uílame Umbelino Gomes, Marcello Filgueira,Diego Pires Gurgel, Lukas Bichler, Meysam Mashhadikarimi,.Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT). 90 (),105234.

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